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Today s knowledge about the human exposure to carcinogenic N-nitroso compounds is based on studies from more than 40 years of research. One of the rst publications that dealt with N-nitroso compounds in food was by Ender et al. (1). The authors described the occurrence of a hepatotoxic factor in herring meal produced from sodium nitrite-preserved herring that was used as feed for sheep. Although appropriate analytical methods were not available yet, the group identi ed N-nitrosodimethylamine (NDMA), obviously present at rather high concentrations in the feed, as the most probable causative agent. The treatment of food with nitrite was suspected to be the causative factor for the formation of N-nitrosamines. As a result of these ndings, a large series of analytical studies to uncover the presence of N-nitroso compounds in food was triggered. The challenging and dif cult analytical detection of N-nitroso compounds was greatly improved with the advent of the highly speci c and ultrasensitive gas chromatographic detector by Fine and Rounbehler (2), called thermal energy analyzer (TEA). It relies on thermal cleavage of the

Investing in application recovery is akin to the message sent out by health management organizations: If you do a good job of early detection and prevention, you won t get too sick. Given that software failures account for a large portion of system failures, your applications need to be sensitive to the different types of faults they ll hit. That s another reason why investments in applications come before investments in clustering software. Why make a bad application failover between hosts, instead of fixing the application Job one is to decide how you ll react to each type of failure. These are cost-time-benefit evaluations, balancing the time required to implement a recovery technique against the cost of having or not having that recovery, with the possible benefit of the automated recovery considered. There s no sense in adding checkpoint features to a database application if it can be easily restarted and the database handles transactional integrity. On the other hand, if an application crash runs the risk of corrupting data or propagating wrong answers, you ll want to invest in taking the necessary steps to keep your data flows clean. We ve broken down recovery techniques into five major categories. We ll provide an overview of these categories here, and then dive into detail on how the most appropriate ones apply to each type of data management service crash, nonfatal system error, and internal logic problem. Detect and retry. Images of Abort, Retry, Fail haunt DOS-literate users. This is the simplest approach, and while it seems obvious, you need to be sure your application tries enough to achieve reconnection to a data service or recovery. In the event of memory exhaustion or

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Process-Induced Food Toxicants: Occurrence, Formation, Mitigation, and Health Risks, Edited by Richard H. Stadler and David R. Lineback Copyright 2009 by John Wiley & Sons, Inc.

network disconnects, for example, it s possible for an application to punt and simply crash, or for it to sleep for a few seconds, try to wait out a short-term memory deficit or network glitch, and then retry the failed call again Patience is sometimes rewarded Gentle shutdown Faced with a case of memory exhaustion that doesn t resolve itself quickly (perhaps another application has a memory leak and has consumed the entire machine), or a floating-point exception that can t be fixed, it s necessary to save state and make sure files are left as consistent as possible User-level applications should try to fail gently, leaving clear messages for users about what happened and what to do next Crash, burn, and restart.

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First publications on the toxicity of N-nitroso compounds (NOCs) in the mid-1950s, identifying N-nitrosodimethylamine (NDMA) as a potent liver toxine and carcinogen GC coupled to a thermal energy analyzer (TEA) or GC/HLPC with high-resolution mass spectrometry In cured and smoked meats and meat products Processing by direct drying techniques (increased NOx exposure) usually equates to higher amounts of NOCs, and initial concerns were raised in the case of beer (malt) NOCs have also been found at trace levels in other foods such as cocoa, cheese, powdered milks and eggs, coffee, instant soups, and spices Classical reaction of an amine or N-nitrosatable amino acid with a nitrosating agent (eg, nitrous acid, formed from nitrite under acidic conditions, or NOx) The pKa value of the amino group is decisive for the nitrosation rate NOC formation at basic conditions is of major importance for industrial/workplace situations.

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